_space_group_crystal_system       'monoclinic'
_space_group_IT_number            15
_space_group_name_H-M_alt         'C 1 2/c 1'

_cell_length_a                    23.2335(12)
_cell_length_b                    15.1665(8)
_cell_length_c                    15.4526(8)
_cell_angle_alpha                 90
_cell_angle_beta                  116.160(2)
_cell_angle_gamma                 90
_cell_volume                      4887.3(4)
_cell_formula_units_Z             8

_diffrn_ambient_temperature       150.0
_diffrn_measurement_device_type   'Bruker APEX-II CCD'
_diffrn_radiation_type            MoK\a
_diffrn_radiation_wavelength      0.71073

_refine_ls_number_parameters      301
_refine_ls_number_reflns          17644
_refine_ls_R_factor_all           0.0388
_refine_ls_R_factor_gt            0.0259

loop_
  _atom_site_label
  _atom_site_type_symbol
  _atom_site_fract_x
  _atom_site_fract_y
  _atom_site_fract_z
  _atom_site_U_iso_or_equiv
  _atom_site_adp_type
  _atom_site_occupancy
  _atom_site_site_symmetry_order
  _atom_site_calc_flag
  _atom_site_refinement_flags_posn
  _atom_site_refinement_flags_adp
  _atom_site_refinement_flags_occupancy
  _atom_site_disorder_assembly
  _atom_site_disorder_group
 Re1 Re 0.40232(2) 0.28706(2) 0.35335(2) 0.00905(1) Uani 1 1 d . . . . .
 Cl1 Cl 0.33367(3) 0.50094(3) 0.19917(4) 0.02594(9) Uani 1 1 d . . . . .
 Cl2 Cl 0.21162(3) 0.19799(4) 0.20290(4) 0.02599(9) Uani 1 1 d . . . . .
 Cl3 Cl 0.51564(3) 0.32059(6) 0.63707(4) 0.03467(13) Uani 1 1 d . . . . .
 Cl4 Cl 0.33238(4) 0.08030(4) 0.44354(6) 0.04047(16) Uani 1 1 d . . . . .
 O1 O 0.53840(7) 0.20874(11) 0.44256(13) 0.0246(3) Uani 1 1 d . . . . .
 O2 O 0.42551(9) 0.33469(12) 0.17808(12) 0.0261(3) Uani 1 1 d . . . . .
 O3 O 0.36498(8) 0.10689(10) 0.25471(11) 0.0225(3) Uani 1 1 d . . . . .
 N1 N 0.42387(7) 0.41569(10) 0.42079(11) 0.0149(2) Uani 1 1 d . . . . .
 N3 N 0.30671(7) 0.34232(9) 0.29560(9) 0.01241(19) Uani 1 1 d . . . . .
 N4 N 0.38825(6) 0.25929(9) 0.48026(9) 0.01184(19) Uani 1 1 d . . . . .
 C1 C 0.48805(8) 0.24035(11) 0.41048(12) 0.0145(2) Uani 1 1 d . . . . .
 C2 C 0.41653(8) 0.31882(11) 0.24424(12) 0.0152(2) Uani 1 1 d . . . . .
 C3 C 0.37719(8) 0.17452(11) 0.29336(12) 0.0141(2) Uani 1 1 d . . . . .
 C4 C 0.42035(9) 0.47900(11) 0.45859(13) 0.0164(3) Uani 1 1 d . . . . .
 C5 C 0.41431(12) 0.55738(15) 0.5076(2) 0.0281(4) Uani 1 1 d . . . . .
 H5A H 0.4066 0.6086 0.4653 0.042 Uiso 1 1 calc GR . . . .
 H5B H 0.4539 0.5663 0.5668 0.042 Uiso 1 1 calc GR . . . .
 H5C H 0.3783 0.5502 0.5238 0.042 Uiso 1 1 calc GR . . . .
 C6 C 0.27272(8) 0.34716(12) 0.19373(11) 0.0152(2) Uani 1 1 d . . . . .
 C7 C 0.28294(10) 0.41423(13) 0.13997(13) 0.0197(3) Uani 1 1 d . . . . .
 C8 C 0.25167(12) 0.41575(16) 0.03960(14) 0.0272(4) Uani 1 1 d . . . . .
 H8 H 0.2611 0.4607 0.0050 0.033 Uiso 1 1 calc R . . . .
 C9 C 0.20690(12) 0.35152(18) -0.00936(14) 0.0304(5) Uani 1 1 d . . . . .
 H9 H 0.1850 0.3529 -0.0778 0.036 Uiso 1 1 calc R . . . .
 C10 C 0.19393(10) 0.28511(17) 0.04112(14) 0.0266(4) Uani 1 1 d . . . . .
 H10 H 0.1625 0.2416 0.0078 0.032 Uiso 1 1 calc R . . . .
 C11 C 0.22736(8) 0.28295(13) 0.14097(13) 0.0185(3) Uani 1 1 d . . . . .
 C12 C 0.21528(10) 0.42249(15) 0.29613(15) 0.0223(3) Uani 1 1 d . . . . .
 H12A H 0.2233 0.4750 0.2662 0.033 Uiso 1 1 calc GR . . . .
 H12B H 0.1998 0.4404 0.3432 0.033 Uiso 1 1 calc GR . . . .
 H12C H 0.1828 0.3857 0.2463 0.033 Uiso 1 1 calc GR . . . .
 C13 C 0.27657(8) 0.37068(11) 0.34644(11) 0.0136(2) Uani 1 1 d . . . . .
 C14 C 0.29832(8) 0.35547(12) 0.44552(12) 0.0154(2) Uani 1 1 d . . . . .
 H14 H 0.2781 0.3891 0.4762 0.018 Uiso 1 1 calc R . . . .
 C15 C 0.34604(8) 0.29706(11) 0.50486(11) 0.0131(2) Uani 1 1 d . . . . .
 C16 C 0.34805(10) 0.27652(14) 0.60154(13) 0.0192(3) Uani 1 1 d . . . . .
 H16A H 0.3404 0.2134 0.6053 0.029 Uiso 1 1 calc GR . . . .
 H16B H 0.3148 0.3105 0.6094 0.029 Uiso 1 1 calc GR . . . .
 H16C H 0.3902 0.2923 0.6528 0.029 Uiso 1 1 calc GR . . . .
 C17 C 0.42886(9) 0.19302(13) 0.54102(13) 0.0180(3) Uani 1 1 d . . . . .
 C18 C 0.49064(11) 0.21139(18) 0.61278(14) 0.0268(4) Uani 1 1 d . . . . .
 C19 C 0.53277(16) 0.1453(3) 0.66456(19) 0.0499(10) Uani 1 1 d . . . . .
 H19 H 0.5745 0.1596 0.7125 0.060 Uiso 1 1 calc R . . . .
 C20 C 0.5136(2) 0.0585(3) 0.6459(2) 0.0597(13) Uani 1 1 d . . . . .
 H20 H 0.5428 0.0128 0.6800 0.072 Uiso 1 1 calc R . . . .
 C21 C 0.4521(2) 0.0369(2) 0.5780(3) 0.0533(11) Uani 1 1 d . . . . .
 H21 H 0.4388 -0.0229 0.5665 0.064 Uiso 1 1 calc R . . . .
 C22 C 0.41011(15) 0.10466(14) 0.52684(18) 0.0302(5) Uani 1 1 d . . . . .

loop_
  _atom_site_aniso_label
  _atom_site_aniso_U_11
  _atom_site_aniso_U_22
  _atom_site_aniso_U_33
  _atom_site_aniso_U_23
  _atom_site_aniso_U_13
  _atom_site_aniso_U_12
 Re1 0.00876(2) 0.00930(2) 0.00924(2) 0.00072(1) 0.00409(2) 0.00059(2)
 Cl1 0.0326(2) 0.01830(18) 0.0300(2) 0.00926(16) 0.0166(2) 0.00498(17)
 Cl2 0.01949(18) 0.0323(2) 0.0229(2) -0.00394(17) 0.00641(16) -0.00904(17)
 Cl3 0.0198(2) 0.0604(4) 0.01670(19) -0.0046(2) 0.00152(16) -0.0087(2)
 Cl4 0.0667(5) 0.0231(2) 0.0461(3) -0.0089(2) 0.0380(3) -0.0233(3)
 O1 0.0131(5) 0.0305(8) 0.0290(7) 0.0080(6) 0.0083(5) 0.0070(5)
 O2 0.0325(8) 0.0319(8) 0.0231(6) 0.0115(5) 0.0205(6) 0.0117(6)
 O3 0.0279(7) 0.0154(5) 0.0216(6) -0.0052(4) 0.0085(5) -0.0019(5)
 N1 0.0148(5) 0.0136(5) 0.0176(5) -0.0012(4) 0.0083(4) -0.0019(4)
 N3 0.0115(4) 0.0152(5) 0.0102(4) 0.0017(4) 0.0045(4) 0.0029(4)
 N4 0.0115(4) 0.0131(5) 0.0111(5) 0.0017(4) 0.0051(4) 0.0008(4)
 C1 0.0123(5) 0.0158(6) 0.0156(6) 0.0021(4) 0.0063(5) 0.0011(5)
 C2 0.0166(6) 0.0161(6) 0.0154(6) 0.0039(5) 0.0093(5) 0.0047(5)
 C3 0.0145(6) 0.0135(6) 0.0133(6) -0.0003(4) 0.0051(5) 0.0002(4)
 C4 0.0159(6) 0.0148(6) 0.0203(7) -0.0031(5) 0.0096(5) -0.0023(5)
 C5 0.0276(9) 0.0207(8) 0.0402(12) -0.0133(8) 0.0188(9) -0.0020(7)
 C6 0.0134(5) 0.0200(7) 0.0116(5) 0.0028(4) 0.0051(5) 0.0064(5)
 C7 0.0220(7) 0.0217(7) 0.0171(7) 0.0077(5) 0.0101(6) 0.0104(6)
 C8 0.0353(10) 0.0327(10) 0.0161(7) 0.0111(7) 0.0135(7) 0.0197(9)
 C9 0.0323(10) 0.0427(12) 0.0118(7) 0.0034(7) 0.0057(7) 0.0203(9)
 C10 0.0189(7) 0.0403(12) 0.0140(7) -0.0040(7) 0.0013(6) 0.0103(7)
 C11 0.0125(6) 0.0271(8) 0.0129(6) -0.0003(5) 0.0028(5) 0.0046(5)
 C12 0.0174(7) 0.0295(9) 0.0210(7) 0.0059(6) 0.0095(6) 0.0121(6)
 C13 0.0120(5) 0.0151(6) 0.0141(5) 0.0012(4) 0.0061(4) 0.0029(4)
 C14 0.0147(6) 0.0186(6) 0.0147(6) 0.0003(5) 0.0082(5) 0.0029(5)
 C15 0.0131(5) 0.0156(6) 0.0117(5) -0.0005(4) 0.0064(4) -0.0011(4)
 C16 0.0211(7) 0.0260(8) 0.0136(6) 0.0018(5) 0.0106(6) 0.0005(6)
 C17 0.0209(7) 0.0206(7) 0.0142(6) 0.0071(5) 0.0093(5) 0.0075(6)
 C18 0.0207(8) 0.0439(12) 0.0143(7) 0.0072(7) 0.0063(6) 0.0126(8)
 C19 0.0439(15) 0.083(2) 0.0208(10) 0.0189(12) 0.0122(10) 0.0440(17)
 C20 0.087(3) 0.061(2) 0.0367(14) 0.0282(14) 0.0330(17) 0.059(2)
 C21 0.104(3) 0.0275(12) 0.0468(16) 0.0220(11) 0.050(2) 0.0337(16)
 C22 0.0542(15) 0.0175(8) 0.0300(10) 0.0101(7) 0.0286(11) 0.0110(9)